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It is interesting to study whether the azobenzene molecular conformational rearrangements can result in changes to bulk phenomena, or even to macroscopic motion. The rst consideration is whether the material expands to an appreciable extent. In monolayers, it is well established that the larger molecular size of the cis isomer leads to a corresponding lateral expansion (Higuchi et al., 1995b), which can modify other bulk properties. For instance, this allows photomodulation of a monolayer s water contact angle (Siewierski et al., 1996) or surface potential (Stiller et al., 1999). Using uorinated azo polymer, good photocontrol (Feng et al., 2001) and photopatterning (Moller et al., 1998) of wettability has been demonstrated. A monolayer of azo-modi ed calixarene, when irradiated with a light gradient, produced a gradient in surface energy suf cient to move a macroscopic oil droplet (Ichimura et al., 2000), suggesting possible applications in micro uidics. Modest photoinduced contact angle changes for thin polymer lms have also been reported (Sarkar et al., 2001). Recently an azobenzene copolymer assembled into polyelectrolyte multilayer showed a modest 21 change in contact angle with UV light irradiation. However, when the same copolymer was assembled onto a patterned substrate, the change in contact angle upon irradiation was enhanced to 701 (Jiang et al., 2005). It is well established that

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A method used for preparation of tiny segments of biological membranes (patch-clamp) is also applied to BLM preparation (Fig 6IOC)..

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Right as the blade market began to take off and numerous vendors entered the game, the Internet bubble burst. As a result, the blade start-up companies struggled, and many disappeared. Others started focusing on niche areas in order to stay in business. RLX focused on HPCC. Egenera focused on financial processing and found substantial success. Amphus focused on management software. Transmeta focused on the low-power niche, sacrificing performance for power management and low power requirements. The InfiniBand players focused on efforts to move all fabrics to InfiniBand. Success during this time came through a variety of niche markets such as imaging, financial tradingfloor projects, military projects requiring portable self-contained rack systems, and even shipboard gambling. In 2004, RLX exited the hardware business, and in 2005 they sold the Control Tower software to HP. Dell, who had entered the market in 2002, did not refresh their product at all during this time. With the market being so soft, blades did not represent a new opportunity for Dell, and served only to cannibalize their existing server market. (As the market began to come back, Dell re-entered in 2004.)

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surface roughness plays a role in contact angle and many systems can be optimized to give rise to a large change in surface properties In layered inorganic systems with intercalated azobenzenes, reversible photochanges in the basal spacing (on the order of 4%) can be achieved (Fujita et al, 1998, 2001) In polymer lms, there is some evidence that the lm thickness increases, as measured by ellipsometry (Shi et al, 1991b) (the refractive index certainly changes [Ivanov et al, 1995], but this is not an unambiguous demonstration of expansion contraction) Experiments that show that external applied pressure tends to hinder photoisomerization (Kleideiter et al, 2000) are related Photocontraction for semicrystalline main-chain azos has been measured (Eisenbach, 1980b; Agolini and Gay, 1970) This photomechanical response presumably occurs because of the shortening of the polymer chains upon trans-cis conversion.

Fig. 6.10 Methods of preparation of bilayer lipid membranes. (A) A Teflon septum with a window of approximately 1 mm2 area divides the solution into two compartments (a). A drop of a lipid-hexane solution is placed on the window (b). By capillary forces the lipid layer is thinned and a bilayer (black in appearance) is formed (c) (P. Mueller, D. O. Rudin, H. Ti Tien and W. D. Wescot). (B) The septum with a window is being immersed into the solution with a lipid monolayer on its surface (a). After immersion of the whole window a bilayer lipid membrane is formed (b) (M. Montal and P. Mueller). (C) A drop of lipid-hexane solution is placed at the orifice of a glass capillary (a). By slight sucking a bubble-formed BLM is shaped (b) (U. Wilmsen, C. Methfessel, W. Hanke and G. Boheim)

However, photoexpansion would seem to be contradicted by positron lifetime experiments that suggest no change in microscopic free volume cavity size during irradiation (Algers et al, 2004) More conclusive experiments are in order The most convincing demonstration of macroscopic motion due to azo isomerization is the mechanical bending and unbending of a free-standing polymer lm (Ikeda et al, 2003; Yu et al, 2003) The macroscopic bending direction may be selected either with polarized light or by aligning the chromophores with rubbing Bending occurs in these relatively thick lms because the free surface (which absorbs light) contracts, whereas the interior of the lm (which is not irradiated owing to the strong absorption of the upper part of the lm) does not contract Because the direction of bending can be controlled with polarized light, the materials enable full directional photomechanical control (Yu et al, 2005).

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The conductivity of membranes that do not contain dissolved ionophores or lipophilic ions is often affected by cracking and impurities. The value for a completely compact membrane under reproducible conditions excluding these effects varies from 10~8 to 10~10 Q" 1 cm"2. The conductivity of these simple 'unmodified' membranes is probably statistical in nature (as a result of thermal motion), due to stochastically formed pores filled with water for an instant and thus accessible for the electrolytes in the solution with which the membrane is in contact. Various active (natural or synthetic) substances

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