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Hamelinck PJ, Huck WTS 2005 Homeotropic alignment on surface initiated liquid crystalline polymer brushes J Mater Chem 15:381 385 Han M, Morino S, Ichimura K 1999 Successive occurrence of biaxial reorientation of azobenzene chromophores of a liquid crystalline polymer induced by linearly polarized light Chem Lett 28:645 646 Han M, Morino S, Ichimura K 2000 Factors affecting in plane and out of plane photoorientation of azobenzene side chains attached to liquid crystalline polymers induced by irradiation with linearly polarized light Macromolecules 33:6360 6371 Hara M, Mizoshita N, Nagano S, Seki T 2007 Chromonic/silica nanohybrids Synthesis and macroscopic alignment Langmuir 23:12350 12355 Ichimura K 2000 Photoalignment of liquid crystal systems Chem Rev 100:1847 1874 Ichimura K, Fujiwara T, Momose M, Matsunaga D 2002 Surface assisted photoalign ment control of lyotropic liquid crystals Part 1 Characterization and photoalignment of aqueous solutions of a water soluble dye as lyotropic liquid crystals.

The activity of the solvent molecule HS in a single-component solvent is constant and is included in ^ H s- The concentration of ions is mostly quite low. For example, self-ionization occurs in water according to the equation 2H 2 O-^H 3 O + + OH~. The conductivity of pure water at 18 C is only 3.8 x 10~8Q"1 cm"1, yielding a degree of self-ionization of 1.4xlO~19. Thus, one H 3 O + or OH~ ion is present for every 7.2 x 108 molecules of water. Some values of Kus a r e listed in Table 1.5 and the temperature dependence of the ion product of water Kw is given in Table 1.6. The H2S+ ion is generally termed a lyonium ion and the S~ ion is termed a lyate ion. The symbol H2S+ (for example H 3 O + , CH3COOH2+, etc.) refers only to a 'proton solvated by a suitable solvent' and does not express either the degree of solvation (solvation number) or the structure. For example, two water molecules form the lyonium ion H 3 O + , termed the oxonium (formerly hydronium or hydroxonium) ion, and the lyate ion OH", termed the hydroxide ion. The existence of the species, H 3 O + , was substantiated as early as in 1924

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Table 1.5 Solvent Acetamide Acetonitrile Acetic acid Hydrofluoric acid Formic acid Hydrogen sulphide Sulphuric acid Ammonia Dimethylsulphoxide Water Ethanol Ethanolamine Formamide Hydrazine Methanol Self-ionization constants of solvents. (According to B. Tremillon) Cation CH 3 CONH 3 CH 3 CNH + CH 3 CO 2 H 2 + H2F+ HCO 2 H 2 + H 3 S 2+ H 3 SO 4 + NH 4 +

J Mater Chem 12:3380 3386 Ichimura K, Momose M, Kudo K, Akiyama H, Ishizuki N 1995 Surface assisted photolithography to form anisotropic dye layers as a new horizon of command surfaces Langmuir 11:2341 2343 Ichimura K, Oh SG, Nakagawa M 2000 Light driven motion of liquids on a photo responsive surface Science 288:1624 1626 Ichimura K, Suzuki Y, Seki T, Hosoki A, Aoki K 1988 Reversible change in alignment mode of nematic liquid crystals regulated photochemically by command surfaces modi ed with an azobenzene monolayer Langmuir 4:1214 1216 Ikeda T 2003 Photomodulation of liquid crystal orientations for photonic applications J Mater Chem 13:2037 2057 Ikeda T, Mamiya J, Yu Y 2007 Photomechanics of liquid crystalline elastomers and other polymers Angew Chem Int Ed Engl 46:506 528 Irie M, editor 2000 Special issue of photochromism: memories and switches Chem Rev 100(5):1683 1890 Kadota S, Aoki K, Nagano S, Seki T 2005.

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Anion CH 3 CONH CH 2 CN CH 3 CO 2 F HCO 2 ~ HS~ HSO 4 HN2~ QH5SOHO C 2 H 5 O~ H 2 NC 2 H 4 OHCONH" N2H3" CH 3 O

Photocontrolled microphase separation of a block copolymer in two dimensions J Am Chem Soc 127:8266 8267 Kadota S, Aoki K, Nagano S, Seki T 2006 Morphological conversions of nanostructures in monolayers of an ABA triblock copolymer having azobenzene moiety Colloids Surf A 284/285:535 541 Kago K, Fuerst M, Matsuoka H, Yamaoka H, Seki T 1999 Direct observation of photoisomerization of polymer monolayer on water surface by X ray re ectometry Langmuir 15:2237 2240 Kato T 2002 Self assembly of phase segregated liquid crystal structures Science 295:2414 2418 Kato T, Frechet JMJ 1989 New approach to mesophase stabilization through hydrogen bonding molecular interactions in binary mixtures J Am Chem Soc 111:8533 8534 Kawashima Y, Nakagawa M, Ichimura K, Seki T 2004 Photo orientation of mesoporous silica materials via transfer from azobenzene containing polymer monolayer J Mater Chem 14:328 335..

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